Chemical fact sheet: Luteolin O-glucuronide

Luteolin O-glucuronide

Basics

Category
Flavone and flavonol derivatives
IUPAC-name
Formula
No formula stored
Exact mass
None g/mol
Molecular weight
462.40000 g/mol
Structure

Sources

In summary, the chemical luteolin O-glucuronide has been analyzed from following sources:

Serratula tinctoria  L.
1st 2nd 3rd

Note that an analysis result in the database may indicate either presence or lack thereof of a chemical in an analyzed sample.

References

  1. K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .
  2. K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .
  3. K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .

Analysis results

Analysis result 1

Detection technique Values Units
[M⁻ H]⁻ 461 m/z
MS²⁻ 285 m/z
MS³⁻ 65
133
151
199 		m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-diode array (DAD), HPLC-UV/Vis
Mass spectrometer description
triple-quadrupole, LC-MSD, ESI MS/MS
Organism
Serratula tinctoria  L.
cultivated
dried
Sample note
The samples were from the Center for Biological Diversity Conservation of the Polish Academy of Sciences Botanical Garden.
Drying methods
lyophilized
Extraction solvents
methanol
Extraction mass/volume-ratio
4 mg/mL
Extraction repeats
1
Extraction time
45 min
Extraction temperature
60 °C
Analysis solvents
MeOH
Detection note
It was found that flavonoid-O-glucuronides react with MeOH in the presence of HCl, forming stable O-methylated derivatives.
References

K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .

Analysis result 2

Detection technique Values Units
[M⁻ H]⁻ 461 m/z
MS²⁻ 285 m/z
MS³⁻ 133 m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-diode array (DAD), HPLC-UV/Vis
Mass spectrometer description
triple-quadrupole, LC-MSD, ESI MS/MS
Organism
Serratula tinctoria  L.
cultivated
dried
Sample note
The samples were from the Center for Biological Diversity Conservation of the Polish Academy of Sciences Botanical Garden.
Drying methods
lyophilized
Extraction solvents
methanol
Extraction mass/volume-ratio
4 mg/mL
Extraction repeats
1
Extraction time
45 min
Extraction temperature
60 °C
Analysis solvents
MeOH
References

K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .

Analysis result 3

Detection technique Values Units
[M⁻ H]⁻ 461 m/z
MS²⁻ 285 m/z
MS³⁻ 133 m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-diode array (DAD), HPLC-UV/Vis
Mass spectrometer description
triple-quadrupole, LC-MSD, ESI MS/MS
Organism
Serratula tinctoria  L.
cultivated
dried
Sample note
The samples were from the Center for Biological Diversity Conservation of the Polish Academy of Sciences Botanical Garden.
Drying methods
lyophilized
Extraction solvents
methanol
Extraction mass/volume-ratio
4 mg/mL
Extraction repeats
1
Extraction time
45 min
Extraction temperature
60 °C
Analysis solvents
MeOH
References

K. Lech, K. Witkoś, and M. Jarosz, "HPLC-UV-ESI-MS/MS identification of the color constituents of sawwort (Serratula tinctoria L.).," Analytical and Bioanalytical Chemistry , vol. 406 , pp. 3703–3708 , DOI: 10.1007/s00216-013-7589-3 .