Chemical fact sheet: Apigenin 7-O-glucoside

The BCDB-database is not an authoritative database. This sheet collates data stored for chemical entry apigenin 7-O-glucoside and its related chemical compound entries cosmosiin .

Apigenin 7-O-glucoside

Basics

Category
Flavone and flavonol derivatives
IUPAC-name
5-hydroxy-2-(4-hydroxyphenyl)-7-((3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)-4H-chromen-4-one
Formula
C21H20O10
Exact mass
432.10560 g/mol
Molecular weight
432.40000 g/mol
Structure
Chemical structure of apigenin 7-O-glucoside
Figure 1.1: Chemical structure of apigenin 7-O-glucoside

Sources

In summary, the chemical apigenin 7-O-glucoside has been analyzed from following sources:

Achillea millefolium  L.
1st 2nd 3rd
Daphne gnidium  L.
1st
Tanacetum balsamita  L.
1st
Tanacetum parthenium  (L.) Sch. Bip.
1st 2nd 3rd
Tanacetum vulgare  L.
1st

Note that an analysis result in the database may indicate either presence or lack thereof of a chemical in an analyzed sample.

References

  1. K. Bączek, O. Kosakowska, J. Przybył, E. Pióro-Jabrucka, R. Costa, L. Mondello, M. Gniewosz, A. Synowiec, and Z. Węglarz, "Antibacterial and antioxidant activity of essential oils and extracts from costmary (Tanacetum balsamita L.) and tansy (Tanacetum vulgare L.).," Industrial Crops and Products , vol. 102 , pp. 154–163 , DOI: 10.1016/j.indcrop.2017.03.009 .
  2. M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .
  3. R. Marques, M. Sousa, M. Oliveira, and M. Melo, "Characterization of weld (Reseda luteola L.) and spurge flax (Daphne gnidium L.) by high-performance liquid chromatography–diode array detection–mass spectrometry in Arraiolos historical textiles.," Journal of Chromatography A , vol. 1216 , pp. 1395–1402 , DOI: 10.1016/j.chroma.2008.12.083 .
  4. G. Zengin, A. Cvetanonović, U. Gašić, A. Stupar, G. Bulut, I. Şenkardes, A. Dogan, K. Sinan, Z. Aumeeruddy-Elalfi, A. Aktumsek, and M. Mahomoodally, "Modern and traditional extraction techniques affect chemical composition and bioactivity of Tanacetum parthenium (L.) Sch. Bip.," Industrial Crops and Products , vol. 146 , pp. 112202 , DOI: 10.1016/j.indcrop.2020.112202 .

Analysis results

Analysis result 1

STD
True
TLC
False
UV/Vis detector description
HPLC-PDA
Mass spectrometer description
Organism
Tanacetum balsamita  L.
cultivated
dried, powdered
Sample note
Plant raw materials, herbs of T. balsamita, at full flowering state; were obtained from the Botanical Garden of Medicinal and Aromatic Plants (Koryciny, Poland). Voucher specimen were deposited at herbarium of Warsaw Universit of Life Sciences, WULS-SGGW, Poland.
Drying methods
air-dried, dark
Drying temperature
35 °C
Extraction solvents
ethanol:water, 40:60, v/v
Extraction mass/volume-ratio
100 mg/mL
Extraction repeats
10
Extraction time
5 h 10 min
Extract liquid storage temperature
-80 °C
Extract drying method
concentration under vacuum
Dried extract storage temperature
4 °C
Analysis solvents
MeOH
References

K. Bączek, O. Kosakowska, J. Przybył, E. Pióro-Jabrucka, R. Costa, L. Mondello, M. Gniewosz, A. Synowiec, and Z. Węglarz, "Antibacterial and antioxidant activity of essential oils and extracts from costmary (Tanacetum balsamita L.) and tansy (Tanacetum vulgare L.).," Industrial Crops and Products , vol. 102 , pp. 154–163 , DOI: 10.1016/j.indcrop.2017.03.009 .

Analysis result 2

STD
True
TLC
False
UV/Vis detector description
HPLC-PDA
Mass spectrometer description
Organism
Tanacetum vulgare  L.
cultivated
dried, powdered
Sample note
Plant raw materials, herbs of T. vulgare, at full flowering state; were obtained from the Botanical Garden of Medicinal and Aromatic Plants (Koryciny, Poland). Voucher specimen were deposited at herbarium of Warsaw Universit of Life Sciences, WULS-SGGW, Poland.
Drying methods
air-dried, dark
Drying temperature
35 °C
Extraction solvents
ethanol:water, 40:60, v/v
Extraction mass/volume-ratio
100 mg/mL
Extraction repeats
10
Extraction time
5 h 10 min
Extract liquid storage temperature
-80 °C
Extract drying method
concentration under vacuum
Dried extract storage temperature
4 °C
Analysis solvents
MeOH
References

K. Bączek, O. Kosakowska, J. Przybył, E. Pióro-Jabrucka, R. Costa, L. Mondello, M. Gniewosz, A. Synowiec, and Z. Węglarz, "Antibacterial and antioxidant activity of essential oils and extracts from costmary (Tanacetum balsamita L.) and tansy (Tanacetum vulgare L.).," Industrial Crops and Products , vol. 102 , pp. 154–163 , DOI: 10.1016/j.indcrop.2017.03.009 .

Analysis result 3

Detection technique Values Units
UV/Vis 332 nm
[M⁻ H]⁻ 431 m/z
MS²⁻ 269 m/z
STD
True
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
methanol
Extraction mass/volume-ratio
16.7 mg/mL
Extraction repeats
2
Extraction time
1 h
Extraction temperature
25 °C
Extract drying method
rotary evaporation
Extract drying temperature
40 °C
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 4

Detection technique Values Units
UV/Vis 332 nm
[M⁻ H]⁻ 431 m/z
MS²⁻ 269 m/z
STD
True
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
water
Extraction mass/volume-ratio
5 mg/mL
Extraction repeats
1
Extraction time
10 min
Extraction temperature
100 °C
Extract drying method
lyophilization, Infusion
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 5

Detection technique Values Units
UV/Vis 332 nm
[M⁻ H]⁻ 431 m/z
MS²⁻ 269 m/z
STD
True
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
water
Extraction mass/volume-ratio
5 mg/mL
Extraction repeats
1
Extraction time
10 min
Extraction temperature
100 °C
Extract drying method
lyophilization, decoction
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 6

Detection technique Values Units
UV/Vis 267
334 		nm
[M⁻ H]⁻ 431 m/z
MS²⁻ 269 m/z
STD
True
TLC
False
UV/Vis detector description
LC-diode array (DAD), PDA
Mass spectrometer description
ESI-MS, ion trap
Organism
Daphne gnidium  L.
wild
Collection dates
2007-5, 2007-6
Sample note
The samples were identified and collected by the researchers.
Extraction solvents
water
Extraction time
1 h
Extraction temperature
100 °C
Analysis solvents
water: MeOH, 8:2
References

R. Marques, M. Sousa, M. Oliveira, and M. Melo, "Characterization of weld (Reseda luteola L.) and spurge flax (Daphne gnidium L.) by high-performance liquid chromatography–diode array detection–mass spectrometry in Arraiolos historical textiles.," Journal of Chromatography A , vol. 1216 , pp. 1395–1402 , DOI: 10.1016/j.chroma.2008.12.083 .

Analysis result 7

Detection technique Values Units
[M⁻ H]⁻ 431.09647 m/z
MS²⁻ 269
311 		m/z
MS³⁻ 151
183
197
255
269 		m/z
STD
True
TLC
False
UV/Vis detector description
UHPLC
Mass spectrometer description
UHPLC-MS, HRMS, LTQ OrbiTrap, UHPLC–LTQ OrbiTrap MS/MS, HESI, heated ESI
Organism
Tanacetum parthenium  (L.) Sch. Bip.
wild
ground, dried
Sample note
The samples were collected in Turkey (Taskopru, Karacaoglu village). Taxonomic spotting was performed at Marmara University, Istanbul, Turkey, voucher number: MARE-19056./ Microwave-assisted extraction (MAE) was performed at 600W microwave power.
Drying methods
air-dried
Extraction solvents
ethanol
Extraction mass/volume-ratio
50 mg/mL
Extraction repeats
1
Extraction time
30 min
Extract drying method
concentration under vacuum
Extract drying temperature
40 °C
Dried extract storage temperature
4 °C
Detection note
MS2 fragments (% base peak): 311 (5), 269 (100); MS3: 269 (30), 255 (100), 197 (45), 183 (30), 151 (20); MS4: 210 (10), 197 (100), 181 (50), 169 (40)
References

G. Zengin, A. Cvetanonović, U. Gašić, A. Stupar, G. Bulut, I. Şenkardes, A. Dogan, K. Sinan, Z. Aumeeruddy-Elalfi, A. Aktumsek, and M. Mahomoodally, "Modern and traditional extraction techniques affect chemical composition and bioactivity of Tanacetum parthenium (L.) Sch. Bip.," Industrial Crops and Products , vol. 146 , pp. 112202 , DOI: 10.1016/j.indcrop.2020.112202 .

Analysis result 8

Detection technique Values Units
[M⁻ H]⁻ 431.09647 m/z
MS²⁻ 269
311 		m/z
MS³⁻ 151
183
197
255
269 		m/z
STD
True
TLC
False
UV/Vis detector description
UHPLC
Mass spectrometer description
UHPLC-MS, HRMS, LTQ OrbiTrap, UHPLC–LTQ OrbiTrap MS/MS, HESI, heated ESI
Organism
Tanacetum parthenium  (L.) Sch. Bip.
wild
ground, dried
Sample note
The samples were collected in Turkey (Taskopru, Karacaoglu village). Taxonomic spotting was performed at Marmara University, Istanbul, Turkey, voucher number: MARE-19056./Sonication of plant-ethanol mixture was done in ultrasonic bath for an hour at 30 °C.
Drying methods
air-dried
Extraction solvents
ethanol
Extraction mass/volume-ratio
40 mg/mL
Extraction repeats
1
Extraction time
1 h
Extraction temperature
30 °C
Extract drying method
concentration under vacuum
Extract drying temperature
40 °C
Dried extract storage temperature
4 °C
Detection note
MS2 fragments (% base peak): 311 (5), 269 (100); MS3: 269 (30), 255 (100), 197 (45), 183 (30), 151 (20); MS4: 210 (10), 197 (100), 181 (50), 169 (40)
References

G. Zengin, A. Cvetanonović, U. Gašić, A. Stupar, G. Bulut, I. Şenkardes, A. Dogan, K. Sinan, Z. Aumeeruddy-Elalfi, A. Aktumsek, and M. Mahomoodally, "Modern and traditional extraction techniques affect chemical composition and bioactivity of Tanacetum parthenium (L.) Sch. Bip.," Industrial Crops and Products , vol. 146 , pp. 112202 , DOI: 10.1016/j.indcrop.2020.112202 .

Analysis result 9

Detection technique Values Units
[M⁻ H]⁻ 431.09647 m/z
MS²⁻ 269
311 		m/z
MS³⁻ 151
183
197
255
269 		m/z
STD
True
TLC
False
UV/Vis detector description
UHPLC
Mass spectrometer description
UHPLC-MS, HRMS, LTQ OrbiTrap, UHPLC–LTQ OrbiTrap MS/MS, HESI, heated ESI
Organism
Tanacetum parthenium  (L.) Sch. Bip.
wild
ground, dried
Sample note
The samples were collected in Turkey (Taskopru, Karacaoglu village). Taxonomic spotting was performed at Marmara University, Istanbul, Turkey, voucher number: MARE-19056./The plant samples were macerated at room temperature at dark for 24 h.
Drying methods
air-dried
Extraction solvents
ethanol
Extraction mass/volume-ratio
50 mg/mL
Extraction repeats
1
Extraction time
1 d
Extraction temperature
20±5 °C
Extract drying method
concentration under vacuum
Extract drying temperature
40 °C
Dried extract storage temperature
4 °C
Detection note
MS2 fragments (% base peak): 311 (5), 269 (100); MS3: 269 (30), 255 (100), 197 (45), 183 (30), 151 (20); MS4: 210 (10), 197 (100), 181 (50), 169 (40)
References

G. Zengin, A. Cvetanonović, U. Gašić, A. Stupar, G. Bulut, I. Şenkardes, A. Dogan, K. Sinan, Z. Aumeeruddy-Elalfi, A. Aktumsek, and M. Mahomoodally, "Modern and traditional extraction techniques affect chemical composition and bioactivity of Tanacetum parthenium (L.) Sch. Bip.," Industrial Crops and Products , vol. 146 , pp. 112202 , DOI: 10.1016/j.indcrop.2020.112202 .

Cosmosiin

Basics

Category
Flavone
IUPAC-name
5-Hydroxy-2-(4-hydroxyphenyl)-7-{[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy}-4H-1-benzopyran-4-one
Formula
C21H20O10
Exact mass
432.10560 g/mol
Molecular weight
No weights stored
Structure
Chemical structure of cosmosiin
Figure 2.1: Chemical structure of cosmosiin

Sources

No links to any potential source for this chemical in the database.

References

  1. K. Bączek, O. Kosakowska, J. Przybył, E. Pióro-Jabrucka, R. Costa, L. Mondello, M. Gniewosz, A. Synowiec, and Z. Węglarz, "Antibacterial and antioxidant activity of essential oils and extracts from costmary (Tanacetum balsamita L.) and tansy (Tanacetum vulgare L.).," Industrial Crops and Products , vol. 102 , pp. 154–163 , DOI: 10.1016/j.indcrop.2017.03.009 .

Analysis results

No analysis results for this entry in the database.