Chemical fact sheet: Quercetin O-hexoside

Quercetin O-hexoside

Basics

Category
Flavone and flavonol derivatives
IUPAC-name
2-(3,4-dihydroxyphenyl)-5,7-dihydroxy-3-((3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)oxy)-4H-chromen-4-one
Formula
No formula stored
Exact mass
464.09548 g/mol
Molecular weight
No weights stored
Structure
Chemical structure of quercetin O-hexoside
Figure 1.1: Chemical structure of quercetin O-hexoside

Sources

In summary, the chemical quercetin O-hexoside has been analyzed from following sources:

Achillea millefolium  L.
1st 2nd 3rd
Filipendula ulmaria  (L.) Maxim.
1st 2nd 3rd

Note that an analysis result in the database may indicate either presence or lack thereof of a chemical in an analyzed sample.

References

  1. M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .
  2. D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .
  3. D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .
  4. D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .

Analysis results

Analysis result 1

Detection technique Values Units
UV/Vis 344 nm
[M⁻ H]⁻ 463 m/z
MS²⁻ 301 m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
methanol
Extraction mass/volume-ratio
16.7 mg/mL
Extraction repeats
2
Extraction time
1 h
Extraction temperature
25 °C
Extract drying method
rotary evaporation
Extract drying temperature
40 °C
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 2

Detection technique Values Units
UV/Vis 344 nm
[M⁻ H]⁻ 463 m/z
MS²⁻ 301 m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
water
Extraction mass/volume-ratio
5 mg/mL
Extraction repeats
1
Extraction time
10 min
Extraction temperature
100 °C
Extract drying method
lyophilization, Infusion
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 3

Detection technique Values Units
UV/Vis 344 nm
[M⁻ H]⁻ 463 m/z
MS²⁻ 301 m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
HPLC-MS/MS
Organism
Achillea millefolium  L.
wild
dried, powdered
Sample note
The wild yarrrow inflorescences and upper leaves were collected by researchers from 50 plants growing in two different grasslands of about one hectare. The gathered material was mixed and made into a unique sample, dried and powdered (20mesh). A voucher specimen was deposited at the Herbarium fo the Excola Superior Agraria de Braganca (BRESA).
Drying methods
lyophilized
Extraction solvents
water
Extraction mass/volume-ratio
5 mg/mL
Extraction repeats
1
Extraction time
10 min
Extraction temperature
100 °C
Extract drying method
lyophilization, decoction
Analysis solvents
water
References

M. Dias, L. Barros, M. Duenas, E. Pereira, A. Carvalho, M. Oliveira, C. Santos-Buelga, and I. Ferreira, "Chemical composition of wild and commercial Achillea millefolium L. and bioactivity of the methanolic extract, infusion and decoction.," Food Chemistry , vol. 141 , no. 4 , pp. 4152–4160 , DOI: 10.1016/j.foodchem.2013.07.018 .

Analysis result 4

Detection technique Values Units
UV/Vis 257
353 		nm
[M⁺ H]⁺ 465 m/z
MS²⁺ 303 m/z
MS³⁺ 109
137
229
257 		m/z
[M⁻ H]⁻ 463 m/z
MS²⁻ 301
343
374 		m/z
MS³⁻ 151
179
255
271 		m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
ESI-MS, HPLC-DAD/MSn
Organism
Filipendula ulmaria  (L.) Maxim.
cultivated
fresh
Sample note
Meadowsweet flowers (Filipendula ulmariae flos) were collected from the Garden of Medical Plants of the Department of Pharmacognosy, Medical University of Lublin. A voucher specimen (No. 09-09-2017_A) was deposited in the Garden of Medical Plants collection. The plant material was identified by Sebastian Granica.
Extraction solvents
boiling water
Extraction repeats
2
Extract drying method
freeze-drying
Analysis solvents
water
Detection note
neutral loss 162
References

D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .

Analysis result 5

Detection technique Values Units
UV/Vis 255
353 		nm
[M⁺ H]⁺ 465 m/z
MS²⁺ 303 m/z
MS³⁺ 153
195
229
247
257 		m/z
[M⁻ H]⁻ 463 m/z
MS²⁻ 151
179
301
343 		m/z
MS³⁻ 151
179
223
255
271 		m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
ESI-MS, HPLC-DAD/MSn
Organism
Filipendula ulmaria  (L.) Maxim.
cultivated
fresh
Sample note
Meadowsweet flowers (Filipendula ulmariae flos) were collected from the Garden of Medical Plants of the Department of Pharmacognosy, Medical University of Lublin. A voucher specimen (No. 09-09-2017_A) was deposited in the Garden of Medical Plants collection. The plant material was identified by Sebastian Granica.
Extraction solvents
boiling water
Extraction repeats
2
Extract drying method
freeze-drying
Analysis solvents
water
Detection note
neutral loss 162
References

D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .

Analysis result 6

Detection technique Values Units
UV/Vis 252
364 		nm
[M⁺ H]⁺ 465 m/z
MS²⁺ 303 m/z
[M⁻ H]⁻ 463 m/z
MS²⁻ 151
179
257
301
343 		m/z
STD
False
TLC
False
UV/Vis detector description
HPLC-DAD
Mass spectrometer description
ESI-MS, HPLC-DAD/MSn
Organism
Filipendula ulmaria  (L.) Maxim.
cultivated
fresh
Sample note
Meadowsweet flowers (Filipendula ulmariae flos) were collected from the Garden of Medical Plants of the Department of Pharmacognosy, Medical University of Lublin. A voucher specimen (No. 09-09-2017_A) was deposited in the Garden of Medical Plants collection. The plant material was identified by Sebastian Granica.
Extraction solvents
boiling water
Extraction repeats
2
Extract drying method
freeze-drying
Analysis solvents
water
References

D. Popowski, K. Pawłowska, J. Piwowarski, and S. Granica, "Gut microbiota-assisted isolation of flavonoids with a galloyl moiety from flowers of meadowsweet, Filipendula ulmaria (L.) Maxim.," Phytochemistry Letters , vol. 30 , pp. 220–223 , DOI: 10.1016/j.phytol.2018.12.003 .